E3 guide for preparation of metallographic specimens. Astm a 262 practice a was used for evaluation of the experimental steel to intergranular. Astm al 93 2016 b8m class 1 astm a262 2015 practice e astm a276 2017 s3160003 a. Astm a262 is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. Welding was performed using the manual gas tungsten arc welding. Description download corrosion intergranular astm a262 comments.
A262 14 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, austenitic stainless steel, copper sulfate, corrosion testing, etch structures, ferric sulfate, intergranular corrosion, nitric acid, oxalic acid. A detailed study of aisi and stainless steels sss has been conducted to correlate the degree of sensitization dos measured by the. Welding duplex stainless steel industry guide lasgroep regio. Th22600fv2stunterteihths527h fa tvorrichtung ths2602 ths260oc330af40 ths260fr5. Is it acceptable for establish the pqr astm a 262 practice e for the material tp321 which contains titanium. Active standard astm a262 developed by subcommittee. The al6xn alloy was designed to be a seawater resistant material and. Uns astm carbon manganese phosphorous sulfur silicon chromium nickel nitrogen s30100. Srinivasan nishi engineers pvt ltd india jan 4, 2010 e mail. As 15 hours is a difficult test period in practice, and is only a minimum. The oxalic acid etch test is rapid and nondestructive, but not quantitative. Every batch of parker 6mo steel is tested for pitting corrosion as per the astm. Astm g48 practicea and astm a262 practicec respectively, for the as cladded and liquid nitrided specimens. Resistant to inter granular corrosion astm a262 practice e.
Once the specimen has been subjected to the solution boil, it is bent through 180. Classification of the structure after a262 practice a analysis will determine if the material is acceptable or if additional testing is required. Standard practice for conditioning containers, packages. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is.
The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular corrosion. Astm news in actuality e 384 and e 92 are not to be married but e38410 will absorb e92 which dealt with macro vickers testing. For annual book of astm standards volume information, refer to the standards document summary page on the astm website. Magnified view of left convex surface and right crosssection of astm a262 practice e tested 304 stainless steel specimen in heat treated condition. Comparison of astm a262 practice a and analytical electron microscopy techniques publication date. Astm a262 practice c 21 determination of the resistance to intergranular corrosion strauss test ml 00221 dinen iso 36512, method a and astm a262 practice e 22 determination of the resistance to pitting corrosion ml 00223 astm g48 method a 23 determination of the freeiron content by ferroxyl test ml 34101 e astm a380. Conducting the single loop slepr and double loop dlepr tests to detect the susceptibility of pitting and igc attack in stainless steel claddings as per astm g5 and astm g108 respectively, for the as cladded and nitrided. The test may be conducted on any object to be tested that can be evacuated and to the other side of which helium or other tracer gas may be applied. Igc test as per astm a 262 02a practice e showing 12 of 2 messages. Corrosion intergranular astm a262 corrosion stainless. Discrepancies between the standard test astm a262 practice e and electrochemical reactivation test method was shown by novak et al. Pdf duplex stainless steel welds and their susceptibility to. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. Where corrosion testing is required for sour service then the following can be subcontracted to other ukas accredited test facilities. Standard test method for liquid penetrant examination se165 identical with astm speci. It is originally a us standard intended to assess the suitability of materials for oilfield equipment where sulphide sulfide stress corrosion cracking may be. Pdf corrosion intergranular astm a262 free download pdf.
Lowtemperature intergranular fracture and grain boundary. An astm designation number identifies a unique version of an astm standard. Standard practices for detecting susceptibility to intergranular attack in. Duplex stainless steel welds and their susceptibility to. Our stainless steel is capable of passing the intergranular corrosion test as per the astm a262 practice. The al6xn alloy was designed to be a seawater resistant material and has since been demonstrated.
Mar 19, 20 the aged specimens were then subjected to astm a262 practice e test in a boiling 16 % h 2 so 4 solution containing 100 gl of cuso 4. Astm a262 intergranular corrosion testing and analysis. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric acid test for detecting susceptibility to intergranular attack was used. Srinivasan nishi engineers pvt ltd india jan 4, 2010 email. The aged specimens were then subjected to astm a262 practice e test in a boiling 16 % h 2 so 4 solution containing 100 gl of cuso 4.
A study on the failure of aisi 304 stainless steel tubes in a. The evaluation consists of the samples being bent in a certain way and after this the surface is inspected. Astm a262 standard practices e test results, a condition 1, b condition 2, c condition 3, d condition 4. As 15 hours is a difficult test period in practice, and is only a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent. Nace mr 0175iso 15156 for corrosion resistant alloys for. Based on the appearance at the bend portion, the specimens were classified into four categories viz. The ballot has to pass the members of e28 and the members of the cos committee. This paper investigates a failure in convection section tubes of a gas heater unit in a. In accordance with astm a262 practice e, iso 36512, din 50914 br, be, am, he, em 19 intergranular corrosion test streichertest sop 4011 in accordance with astm a262 practice b, astm g28 br, be, am, he, em 20 intergranular corrosion test hueytest sop 4012 in accordance with astm a262 practice c, iso 36511 br, be. The astm a262 testing specification contains five unique intergranular corrosion tests. Duplex stainless steel welds and their susceptibility to intergranular corrosion.
However, epa would not accept the limited asbestos screen i. Repeatability and reproducibility of compression strength. A range of corrosion tests can be carried out inhouse including. Duplex stainless steels 97, maastricht, the netherlands, october 1997. Application and interpretation, astm manual series mnl 20, second edition. Astma262 standard practices for detecting susceptibility. The microstructure evolution and its effect on corrosion properties of 18cr12ni2,5mo steel. Astme498 your online library of us and international standards. Method a and astm a262 practice e 22 determination of the resistance to pitting corrosion ml 00223 astm g48 method a 23 determination of the freeiron content by ferroxyl test ml 34101 e astm a380 24 determination of the ferrite deltaferrite content ml 00302 e in house method astm e562 25 metal products metallographic researchml 00300 astm. Suppression of intergranular corrosion of 304 ss through laser. Astm a262 method e is sometimes called the strauss test, and is the same as iso 36512 method a, except for the duration.
Astm a262 practice e strauss test this procedure is conducted to determine the susceptibility of austenitic stainless steel to inter granular attack associated with the precipitation of chromiumrich carbides. Astm g48 practice a and astm a262 practice c respectively, for the as cladded and liquid nitrided specimens. The etch structure types used to classify the specimens are. A380a380m practice for cleaning, descaling, and passivation of stainless steel parts, equipment, and systems. Modified astm a262 standard practices ecoppercopper sulfate sulfuric acid test for detecting. Automated image analysis software for assessing banding or orientation of microstructures in dual phase steel. These practices include five intergranular corrosion tests, namely. Welding was performed using the manual gas tungsten arc welding gtaw. The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular. Report corrosion intergranular astm a262 please fill this form, we will try to respond as.
The broad field of welding parameters for bohler cn 229 nfd permits universal application in a very wide range of wall. They observed that the reactivation method detects both continuous and local chromium depleted region in the steel structure, however acid test exposes only continuous depletion zones leading. Astm a262 practice c stac spec 53961 astm a262 practice d astm a262 practice e. For annual book of astm approved in last previous edition approved in as e 01. Tp 904 l a sa 269 a262 practice e s 31254 a sa 2 s 31803 a sa 789 p.
Duplex stainless steels 97, maastricht, the netherlands, october. Streicher test astm a262 practice b generally used for stainless steel and nickel alloys, the streicher test involves boiling the specimen in a ferric sulfate sulfuric acid solution for 24120 hours and evaluating the results. Comparison of astm a262 practice a and analytical electron microscopy techniques b. Standard practices for detecting susceptibility to. In accordance with astm b117, astm b 368, astm g 85, din 50021, iso 10289, iso 9227, nen 10068 br, am 18 intergranular corrosion test strausstest sop 4010 in accordance with astm a262 practice e, iso 36512, din 50914 br, be, am, he, em 19 intergranular corrosion test streichertest sop 4011 in accordance with astm a262 practice b. Practice ecoppercopper sulfatesulfuric acid test for detecting. Uns astm carbon manganese phosphorous sulfur silicon chromium nickel nitrogen s30100 301 0. Tts diagram for aisi type 316 austenitic stainless steel established according to the test astm a262 practice a. Characteristics and properties of stainless steel 3. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric. The huey test works astm a262 practice e to analyze chromium depleted regions and intermetallic astm a262 practice e, such as sigma phase, lractice is also used for materials in strongly oxidizing astm a262 practice e such as nitric acid. Pdf duplex stainless steels dss as alternatives to conventional austenitic.
Effect of carbon content on eddy current response to. These specimens will have low corrosion rates in certain corrosion tests and therefore can be eliminated screened from testing as acceptable. What is astm a262 intergranular corrosion test igc china. They are nondestructive testing methods for detecting discontinuities that are open to the surface such as cracks, seams, laps, cold shuts. A370 test methods and definitions for mechanical testing of steel products. Test intergranular corrosion o spindle mm length of period h 15 result of visual inspection at 20 x magnification after bend test absence of cracks heat treatment before test sensitization bend angle 0 produced without class 111 ozone depleting substances. Standard practice for liquid penetrant examination1. E 01 standard practice for assessing the degree of bandin. Standards volume information, refer to the standards. Determination of susceptibility to intergranular corrosion. Two test methods namely a modified astm a262 and a modified double loop electrochemical potentiokinetic reactivation dlerp test were employed to determine the susceptibility to igc. Pdf duplex stainless steel welds and their susceptibility. Astm a262 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
Astme498 standard practice for leaks using the mass. This standard covers the practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Astm a26215, standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, astm international, west conshohocken. Astme498 standard practice for leaks using the mass spectrometer leak detector or. Astm a262 practice a screening method has been used as advised by aydogdu and aydinol 2006 to know the susceptibility of the material towards intergranular corrosion. Grain boundary chemistry is known to be a critical. We report a specific time temperature heat treatments that result in brittle intergranular fracture of type 304 stainless steel by impact at liquid nitrogen temperature, by auger electron spectroscopy aes of four sensitized heats of the embrittled grain boundaries and icy the results of a corrosion test, %stm a262 practice e and c, on. A study on the failure of aisi 304 stainless steel tubes in a gas. Copper copper sulfate 16% sulfuric acid, astm a262 practice e strauss test this procedure is conducted to determine the susceptibility of austenitic stainless steel to inter granular attack associated with the precipitation of chromiumrich carbides. The microstructure evolution and its effect on corrosion properties of 18cr12ni2,5mo steel annealed at 500900c 126 in stainless steels refers to their susceptibility to intergranular corrosion resulting from microstructural changes.
Nace mr 0175iso 15156 is a materials standard issued by the national association of corrosion engineers. Astm a262 method c huey test is the same as that specified in iso 36511 not listed here. Astm a262 astm b117 salt spray test astm b368 cass test astm g85 astm g85 a1 astm g85 a2 astm g85 a3 astm g85 a4 astm g85 a5 chemical testing corrosion testing metallography. Al6xn alloy uns n08367 is a low carbon, high purity, nitrogenbearing superaustenitic stainless alloy. Oct 15, 2011 our client specification is silent about the igc test for the material astm a 312 tp321.
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